Pulse and Fourier transform NMR; introduction to theory and methods
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| Author / Creator: | Farrar, Thomas C. (Thomas Clark), 1933- |
|---|---|
| Imprint: | New York, Academic Press, 1971. |
| Description: | xiv, 115 p. illus. 24 cm. |
| Language: | English |
| Subject: | |
| Format: | Print Book |
| URL for this record: | http://pi.lib.uchicago.edu/1001/cat/bib/1047308 |
Table of Contents:
- Preface
- Acknowledgments
- Symbols and Abbreviations
- 1. Basic Concepts in NMR
- 1.1. Relaxation and Nuclear Magnetic Energy Levels
- 1.2. Some Basic Properties of Vectors
- 1.3. Nuclear Precession
- 1.4. The Bloch Equations
- 1.5. The Rotating Frame of Reference
- 1.6. Magnetization in the Rotating Frame
- 1.7. Fourier Analysis and Fourier Transformation
- 2. Free Induction and Spin Echoes
- 2.1. Free Induction Decay
- 2.2. Measurement of T1
- 2.3. Measurement of T2 by the Spin-Echo Method
- 2.4. The Carr-Purcell Technique
- 2.5. The Meiboom-Gill Method
- 2.6. Fourier Transform Methods
- 2.7. Weak Pulses and Selective Relaxation Measurements
- 2.8. Summary of Basic Pulse Methods
- 3. Instrumentation
- 3.1. The Pulsed NMR Spectrometer
- 3.2. The NMR Sample Probe
- 3.3. The rf Gate, Pulse Programmer, and rf Transmitter
- 3.4. The Amplification and Detection System
- 3.5. Systematic Errors in Pulsed NMR Instruments
- 4. Relaxation Mechanisms
- 4.1. Frequency Distribution of Molecular Motions
- 4.2. Spin-Lattice Interactions
- 4.3. Dipole-Dipole Relaxation
- 4.4. Quadrupole Relaxation
- 4.5. Relaxation via Chemical Shift Anisotropy
- 4.6. Scalar Relaxation
- 4.7. Spin-Rotation Relaxation
- 4.8. Summary of Relaxation Mechanisms
- 5. Fourier Transform NMR
- 5.1. Use of the FT Method in Multispin Systems
- 5.2. Instrumental Requirements
- 5.3. Computer Requirements
- 5.4. Effect of ?1 on Signal/Noise Improvement
- 5.5. Multiple-Pulse Techniques
- 5.6. Transient Species; Measurement of Relaxation Times
- 5.7. Stochastic Excitation
- 6. Rotating Frame Experiments
- 6.1. Transient Nutations
- 6.2. Rotary Spin Echoes
- 6.3. Forced Transitory Precession; "Spin Locking"
- 6.4. Waugh Pulse Sequences
- 7. Selected Applications
- 7.1. Molecular Diffusion
- 7.2. Chemical Rate Processes
- 7.3. Molecular Dynamics
- References
- Subject Index
