Supercritical antisolvent precipitation process : fundamentals, applications and perspectives /
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| Author / Creator: | Santos, Diego T., author. |
|---|---|
| Imprint: | Cham, Switzerland : Springer, [2019] |
| Description: | 1 online resource (xviiiI, 82 pages) |
| Language: | English |
| Series: | SpringerBriefs in Applied Sciences and Technology, 2191-530X SpringerBriefs in applied sciences and technology, |
| Subject: | |
| Format: | E-Resource Book |
| URL for this record: | http://pi.lib.uchicago.edu/1001/cat/bib/11981560 |
Table of Contents:
- Intro; Introduction; Contents; About the Authors; 1 A Detailed Design and Construction of a Supercritical Antisolvent Precipitation Equipment; 1.1 Introduction; 1.2 Materials and Methods; 1.2.1 Unit Structure; 1.2.2 Equipment and Materials; 1.3 Results and Discussion; 1.3.1 SAS Unit Operation Procedure; 1.4 Conclusions; References; 2 Effect of Process Conditions on the Morphological Characteristics of Particles Obtained by Supercritical Antisolvent Precipitation; 2.1 Introduction; 2.2 Materials and Methods; 2.2.1 Materials; 2.2.2 Experimental Procedure
- 2.2.3 Experiment Design and Statistical Analysis2.2.4 Analysis and Characterization; 2.3 Results and Discussion; 2.3.1 Influence of the Operating Conditions on the Precipitation Yield; 2.3.2 Influence of Operating Conditions on Residual Organic Solvent Content in the Micronized Particles; 2.3.3 Influence of Operating Conditions on Morphology; 2.3.4 Selecting Appropriate Conditions; 2.4 Conclusions; References; 3 Precipitation of Particles Using Combined High Turbulence Extraction Assisted by Ultrasound and Supercritical Antisolvent Fractionation; 3.1 Introduction; 3.2 Materials and Methods
- 3.2.1 Raw Material3.2.2 Experimental; 3.2.3 Chemical Composition; 3.2.4 Scanning Electron Microscopy; 3.3 Results and Discussion; 3.3.1 Global Precipitation Yield and Particle Distribution in SAF System; 3.3.2 Total Phenolics and Bixin Distribution in SAF System; 3.3.3 Scanning Electron Microscopy; 3.4 Conclusions; References; 4 Recent Developments in Particle Formation with Supercritical Fluid Extraction of Emulsions Process for Encapsulation; 4.1 Introduction; 4.2 Supercritical Fluid Extraction of Emulsions (SFEE); 4.2.1 SFEE Procedures; 4.2.2 Applications
- 4.2.3 Effects of Operational Conditions in SFEE Process4.3 Concluding Remarks; References; 5 Supercritical Fluid Extraction of Emulsion Obtained by Ultrasound Emulsification Assisted by Nitrogen Hydrostatic Pressure Using Novel Biosurfactant; 5.1 Introduction; 5.2 Materials and Methods; 5.2.1 Materials; 5.2.2 Oily Bixin-Rich Extract Production; 5.2.3 Emulsion Preparation and Characterization; 5.2.4 Supercritical Fluid Extraction of Emulsions (SFEE) Process Description; 5.2.5 SFEE Product Characterization; 5.3 Results and Discussion; 5.4 Conclusions; References
- 6 Economical Effects of Supercritical Antisolvent Precipitation Process Conditions6.1 Introduction; 6.2 Materials and Methods; 6.2.1 Materials; 6.2.2 Experimental Procedure; 6.2.3 Determination of Energy Cost Per Unit of Manufactured Product; 6.2.4 Design of the Experiment and Statistical Analysis; 6.3 Results and Discussion; 6.4 Conclusions; References