Spectrometric identification of organic compounds.
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| Author / Creator: | Silverstein, Robert M. (Robert Milton), 1916-2007 |
|---|---|
| Edition: | 7th ed. |
| Imprint: | Hoboken, NJ : Wiley, c2005. |
| Description: | x, 502 p. ; 29 cm. |
| Language: | English |
| Subject: | |
| Format: | Print Book |
| URL for this record: | http://pi.lib.uchicago.edu/1001/cat/bib/5574642 |
Table of Contents:
- Chapter 1. Mass Spectrometry
- 1.1. Introduction
- 1.2. Instrumentation
- 1.3. Ionization Methods
- 1.4. Mass Analyzers
- 1.5. Interpretation of El Mass Spectra
- 1.6. Mass Spectra of Some Chemical Classes
- Chapter 2. Infrared Spectrometry
- 2.1. Introduction
- 2.2. Theory
- 2.3. Instrumentation
- 2.4. Sample Handling
- 2.5. Interpretations of Spectra
- 2.6. Characteristic Group Absorption of Organic Molecules
- Chapter 3. Proton Magnetic Resonance Spectrometry
- 3.1. Introduction
- 3.2. Theory
- 3.3. Instrumentation and Sample Handling
- 3.4. Chemical Shift
- 3.5. Spin Coupling, Multiplets, Spin Systems
- 3.6. Protons on Oxygen, Nitrogen, and Sulfur Atoms. Exchangeable Protons
- 3.7. Coupling of Protons to Other Important Nuclei ( 19 F, E, 31 P, 29 Si, and 13 C
- 3.8. Chemical Shift Equivalence
- 3.9. Magnetic Equivalence (Spin-Coupling Equivalence)
- 3.10. AMX, ABX, and ABC Rigid Systems with Three Coupling Constants
- 3.11. Confirmationally Mobile, Open-Chain Systems. Virtual Coupling
- 3.12. Chirality
- 3.13. Vicinal and Geminal Coupling
- 3.14. Low-Range Coupling
- 3.15. Selective Spin Decoupling. Double Resonance
- 3.16. Nuclear Overhauser Effect, Difference Spectrometry, 1H 1H Proximity Through Space
- Chapter 4. Carbon-13 NMR Spectrometry
- 4.1. Introduction
- 4.2. Theory
- 4.3. Interpretation of a Simple 13 C Spectrum: Diethyl Phthalate
- 4.4. Quantitative 13 C Analysis
- 4.5. Chemical Shift Equivalence
- 4.6. DEPT
- 4.7. Chemical Classes and Chemical Shifts
- Chapter 5. Correlation NMR Spectrometry; 2-D NMR
- 5.1. Introduction
- 5.2. Theory
- 5.3. Correlation Spectrometry
- 5.4. Ipsenol: 1 H- 1 H COSY
- 5.5. Caryophyllene Oxide
- 5.6. 13 C- 13 C Correlations: Inadequate
- 5.7. Lactose
- 5.8. Relayed Coherence Transfer: TOCSY
- 5.9. HMQC - TOCSY
- 5.10. ROESY
- 5.11. VGSE
- 5.12. Gradient Field NMR
- Chapter 6. NMR Spectrometry of Other Important Spin 1/2 Nuclei
- 6.1. Introduction
- 6.2. 15 N Nuclear Magnetic Resonance
- 6.3. 19 F Nuclear Magnetic Resonance
- 6.4. 29 Si Nuclear Magnetic Resonance
- 6.5. 31 P Nuclear Magnetic Resonance
- 6.6. Conclusion
- Chapter 7. Solved Problems
- 7.1. Introduction
- Chapter 8. Assigned Problems
- 8.1. Introduction
